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The peptide could be degraded, the water could be contaminated, or the vial temperature may have caused precipitation

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10.1016/s0091-679x(01)65006-4 4 CatanzaroD.FilippiniR.VianelloC.CarraraM.RagazziE.MontopoliM

Colchicine, a classical microtubule inhibitor, binds to tubulin and blocks microtubule polymerization
